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- ElectrochemicalImpedanceSpectroscopy + (Electrochemical measurement method of the … Electrochemical measurement method of the complex impedance of an electrochemical system as a function of the frequency of a small amplitude (normally 5 to 10 mV) sinusoidal voltage perturbation superimposed on a fixed value of applied potential or on the open circuit potential.otential or on the open circuit potential.)